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X-Ray Structure Determination: A Practical Guide, 2nd EditionCatalog #: 12-223
G.H. Stout, L.H. Jensen (1989) 480 pp.
This book is available only with PRINT ON DEMAND with a 3-5 day lead time with NO returns accepted.
Closely follows an actual structural determination. After some introductory material on the nature of x-rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x-ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the “phase” problems, the principal difficulty in x-ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.